Table 3. Temperature program for microwave digestion.
|
Steps |
Target temp. (°C) |
Pressure limit (bar) |
Ramp time (min) |
Hold time (min) |
Power limit (%) |
|
1 |
140 |
35 |
10 |
2 |
80 |
|
2 |
195 |
35 |
3 |
20 |
100 |
|
3 |
50 |
35 |
1 |
20 |
0 |